3er3: Difference between revisions

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New page: left|200px<br /><applet load="3er3" size="450" color="white" frame="true" align="right" spinBox="true" caption="3er3, resolution 2.0Å" /> '''THE ACTIVE SITE OF AS...
 
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[[Image:3er3.jpg|left|200px]]<br /><applet load="3er3" size="450" color="white" frame="true" align="right" spinBox="true"
caption="3er3, resolution 2.0&Aring;" />
'''THE ACTIVE SITE OF ASPARTIC PROTEINASES'''<br />


==Overview==
==The active site of aspartic proteinases==
The active site of the aspartic proteinase, endothiapepsin, has been, defined by X-ray analysis and restrained least-squares refinement at 2.1 A, resolution with a crystallographic agreement value of 0.16. The, environments of the two catalytically important aspartyl groups are, remarkably similar and the contributions of the NH2- and COOH-terminal, domains to the catalytic centre are related by a local 2-fold axis. The, carboxylates of the aspartyls share a hydrogen bond and have equivalent, contacts to a bound water molecule or hydroxonium ion lying on the local, diad. The main chains around 32 and 215 are connected by a novel, interaction involving diad-related threonines. It is suggested that the, two pKa values of the active site aspartyls arise from a structure not, unlike that in maleic acid with a hydrogen-bonded intermediate species and, a dicarboxylate characterised by electrostatic repulsions between the two, negatively charged groups.
<StructureSection load='3er3' size='340' side='right'caption='[[3er3]], [[Resolution|resolution]] 2.00&Aring;' scene=''>
== Structural highlights ==
<table><tr><td colspan='2'>[[3er3]] is a 1 chain structure with sequence from [https://en.wikipedia.org/wiki/Cryphonectria_parasitica Cryphonectria parasitica]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=3ER3 OCA]. For a <b>guided tour on the structure components</b> use [https://proteopedia.org/fgij/fg.htm?mol=3ER3 FirstGlance]. <br>
</td></tr><tr id='method'><td class="sblockLbl"><b>[[Empirical_models|Method:]]</b></td><td class="sblockDat" id="methodDat">X-ray diffraction, [[Resolution|Resolution]] 2&#8491;</td></tr>
<tr id='ligand'><td class="sblockLbl"><b>[[Ligand|Ligands:]]</b></td><td class="sblockDat" id="ligandDat"><scene name='pdbligand=0EL:6-AMMONIO-N-[(2R,4R,5R)-5-{[N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANYL-3-(1H-IMIDAZOL-3-IUM-4-YL)-L-ALANYL]AMINO}-6-CYCLOHEXYL-4-HYDROXY-2-(2-METHYLPROPYL)HEXANOYL]-L-NORLEUCYLPHENYLALANINE'>0EL</scene></td></tr>
<tr id='resources'><td class="sblockLbl"><b>Resources:</b></td><td class="sblockDat"><span class='plainlinks'>[https://proteopedia.org/fgij/fg.htm?mol=3er3 FirstGlance], [http://oca.weizmann.ac.il/oca-bin/ocaids?id=3er3 OCA], [https://pdbe.org/3er3 PDBe], [https://www.rcsb.org/pdb/explore.do?structureId=3er3 RCSB], [https://www.ebi.ac.uk/pdbsum/3er3 PDBsum], [https://prosat.h-its.org/prosat/prosatexe?pdbcode=3er3 ProSAT]</span></td></tr>
</table>
== Function ==
[https://www.uniprot.org/uniprot/CARP_CRYPA CARP_CRYPA]
== Evolutionary Conservation ==
[[Image:Consurf_key_small.gif|200px|right]]
Check<jmol>
  <jmolCheckbox>
    <scriptWhenChecked>; select protein; define ~consurf_to_do selected; consurf_initial_scene = true; script "/wiki/ConSurf/er/3er3_consurf.spt"</scriptWhenChecked>
    <scriptWhenUnchecked>script /wiki/extensions/Proteopedia/spt/initialview03.spt</scriptWhenUnchecked>
    <text>to colour the structure by Evolutionary Conservation</text>
  </jmolCheckbox>
</jmol>, as determined by [http://consurfdb.tau.ac.il/ ConSurfDB]. You may read the [[Conservation%2C_Evolutionary|explanation]] of the method and the full data available from [http://bental.tau.ac.il/new_ConSurfDB/main_output.php?pdb_ID=3er3 ConSurf].
<div style="clear:both"></div>
<div style="background-color:#fffaf0;">
== Publication Abstract from PubMed ==
The active site of the aspartic proteinase, endothiapepsin, has been defined by X-ray analysis and restrained least-squares refinement at 2.1 A resolution with a crystallographic agreement value of 0.16. The environments of the two catalytically important aspartyl groups are remarkably similar and the contributions of the NH2- and COOH-terminal domains to the catalytic centre are related by a local 2-fold axis. The carboxylates of the aspartyls share a hydrogen bond and have equivalent contacts to a bound water molecule or hydroxonium ion lying on the local diad. The main chains around 32 and 215 are connected by a novel interaction involving diad-related threonines. It is suggested that the two pKa values of the active site aspartyls arise from a structure not unlike that in maleic acid with a hydrogen-bonded intermediate species and a dicarboxylate characterised by electrostatic repulsions between the two negatively charged groups.


==About this Structure==
The active site of aspartic proteinases.,Pearl L, Blundell T FEBS Lett. 1984 Aug 20;174(1):96-101. PMID:6381096<ref>PMID:6381096</ref>
3ER3 is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/ ]. Active as [http://en.wikipedia.org/wiki/Hydrolase Hydrolase], with EC number [http://www.brenda-enzymes.info/php/result_flat.php4?ecno=3.4.21.103, 3.4.23.18, 3.4.23.28 and 3.4.23.30 3.4.21.103, 3.4.23.18, 3.4.23.28 and 3.4.23.30] Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=3ER3 OCA].


==Reference==
From MEDLINE&reg;/PubMed&reg;, a database of the U.S. National Library of Medicine.<br>
The active site of aspartic proteinases., Pearl L, Blundell T, FEBS Lett. 1984 Aug 20;174(1):96-101. PMID:[http://ispc.weizmann.ac.il//pmbin/getpm?pmid=6381096 6381096]
</div>
[[Category: Hydrolase]]
<div class="pdbe-citations 3er3" style="background-color:#fffaf0;"></div>
[[Category: Single protein]]
[[Category: Al-Karadaghi, S.]]
[[Category: Blundell, T.L.]]
[[Category: Cooper, J.B.]]
[[Category: Hoover, D.]]
[[Category: Veerapandian, B.]]
[[Category: hydrolase (acid proteinase)]]


''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Tue Nov 20 19:41:19 2007''
==See Also==
*[[Pepsin|Pepsin]]
== References ==
<references/>
__TOC__
</StructureSection>
[[Category: Cryphonectria parasitica]]
[[Category: Large Structures]]
[[Category: Al-Karadaghi S]]
[[Category: Blundell TL]]
[[Category: Cooper JB]]
[[Category: Hoover D]]
[[Category: Veerapandian B]]

Latest revision as of 08:13, 23 October 2024

The active site of aspartic proteinases

3er3, resolution 2.00Å

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